Twenty Five Years of the Laboratory for the Chemical and Analytical Control of the Federal State Budgetary Establishment «27 Scientific Centre» of the Ministry of Defence of the Russian Federation

The Convention on the prohibition of the development, production, stockpiling and use of chemical weapons and on their destruction (CWC) stipulates the realization of the detailed procedure for the verification of the implementation of all its provisions, including the analytical control of the presence of the prohibited substances in samples, taken during the inspections of the sites of alleged development of chemical weapons (CW). In 1992 the Laboratory for the chemical and analytical control of the Military academy of radiological, chemical and biological defence named after Marshal of the Soviet Union S.K. Timoshenko has been created, and from the very beginning it participates in the above mentioned verification programme. Since 2006 the Laboratory operates within the framework of the federal state budgetary establishment «27 Scientific Centre» of the Ministry of Defence of the Russian Federation. As a result of the successful performance in the OPCW`s (the Organisation for the Prohibition of Chemical Weapons) Official Inter-Laboratory Proficiency Testing Programme, in 2000 the Laboratory has been awarded the status of «designated» (a type of OPCW`s accreditation). It has been certified to perform independent analysis of authentic samples, taken from the sites of international inspections and transferred off-site in accordance with the relevant provisions of the CWC. To date, the OPCW has organized 42 official OPCW Proficiency Tests for the analysis of environmental and technological samples, and two official OPCW Biomedical Proficiency Tests. In 2016, together with the accreditation for the analysis of environmental and technological samples, valid since 2000, the Laboratory of the «27 Scientific Centre» of the Ministry of Defence of the Russian Federation has been designated for the analysis of authentic biomedical samples. During its 25 years of existence, the Laboratory has been successfully solving the problems of the analysis of composite objects during the investigations into the alleged use of chemical weapons, as well as of the analysis of samples, taken from the burial sites for abandoned chemical weapons and from the territories of their former production facilities.

1. Convention on the Prohibition of the Development, Production, Stockpiling and Use of Chemical Weapons and on their Destruction. Organisation for the Prohibition of Chemical Weapons (OPCW), The Hague, The Netherlands, 1997. 179 p.

2. Black R. M. Development, historical use and properties of chemical warfare agents // Chemical Warfare Toxicology, V. 1: Fundamental Aspects, Issues in Toxicology № 27 / Eds. Worek F., Jenner J., Thiermann H. The Royal Society of Chemistry, Cambridge, UK, 2016, Chapter 1, P. 1–28.

3. Chemical Weapons Convention Chemicals Analysis: Sample Collection, Preparation and Analytical Methods / Ed. Mesilaakso M. Chichester, UK: John Wiley & Sons Ltd, 2005.

4. Final Evaluation of Results. First Official OPCW/ PTS Inter-Laboratory Comparison Test: Proficiency Test 18 March 1997. Provisional Technical Secretariat. Preparatory for the Organisation for the Prohbition of Chemical Weapons, OPCW, The Hague, 1997.

5. Soderstrom M.T., Bjork H., Hakkinen V.M. A., Kostiainen O., Kuitunen M.–L., Rautio M. Identification of compounds relevant to the chemical weapons convention using selective gas chromatography detectors, gas chromatographymass-spectrometry and gas chromatography-Fourier transform infrared spectroscopy in an international trial proficiency test // J. Chromatogr. A. 742 (1996). P. 191–203.

6. OPCW Technical Secretariat. Note by the DirectorGeneral Designation of laboratories for the analysis of authentic samples: retention of designation status. Technical Secretariat, OPCW, 1998.

7. Dubey V., Velikeloth S., Sliwakowski M., Mallard G. Official Proficiency Tests of the Organisation of the Prohibition of Chemical Weapons: Current Status and Future Direction // Accred. Qual. Assur. 2009 V. 14 P. 431–437.

8. Organisation for the Prohibition of Chemical Weapons. Standard Operating Procedure for the organisation of the OPCW Proficiency Tests, Quality Management System Document No. QDOC/LAB/SOP/PT01 Issue 2, Revision 3 (April 2014).

9. Organisation for the Prohibition of Chemical Weapons. Work instruction for the preparation of samples for OPCW Proficiency Tests, Quality Management System Document № . QDOC/LAB/WI/PT02 Issue 2, Revision 3 (April 2014).

10. Organisation for the Prohibition of Chemical Weapons. Work instruction for the for the evaluation of the results of OPCW Proficiency Tests, Quality Management System Document № . QDOC/LAB/WI/PT03 Issue 3, Revision 1 (April 2014).

11. Organisation for the Prohibition of Chemical Weapons. Work instruction for the reporting of the results of the OPCW Proficiency Tests, Quality Management System Document № . QDOC/LAB/WI/PT04 Issue 1, Revision 3 (April 2014).